(2015). Spectral, Thermal ,Voltammetric and Biological Studies on Mn(Ii),Fe(II,III), Co(II), Cu(II) and Zn(II) With Cefazolin Antibiotic. test, 44(1), 13-26. doi: 10.21608/aunj.2015.222234
. "Spectral, Thermal ,Voltammetric and Biological Studies on Mn(Ii),Fe(II,III), Co(II), Cu(II) and Zn(II) With Cefazolin Antibiotic". test, 44, 1, 2015, 13-26. doi: 10.21608/aunj.2015.222234
(2015). 'Spectral, Thermal ,Voltammetric and Biological Studies on Mn(Ii),Fe(II,III), Co(II), Cu(II) and Zn(II) With Cefazolin Antibiotic', test, 44(1), pp. 13-26. doi: 10.21608/aunj.2015.222234
Spectral, Thermal ,Voltammetric and Biological Studies on Mn(Ii),Fe(II,III), Co(II), Cu(II) and Zn(II) With Cefazolin Antibiotic. test, 2015; 44(1): 13-26. doi: 10.21608/aunj.2015.222234

Spectral, Thermal ,Voltammetric and Biological Studies on Mn(Ii),Fe(II,III), Co(II), Cu(II) and Zn(II) With Cefazolin Antibiotic

Assiut University Journal of Multidisciplinary Scientific Research
Volume 44, Issue 1, June 2015, Pages 13-26    PDF (1.09 M)
Document Type: Novel Research Articles
DOI: 10.21608/aunj.2015.222234
Abstract
The following complexes of cefazolin(HCefaz) antibiotic were synthesized and investigated: [M(Cefaz)2].xH2O where M=Mn(II),Co(II) ,Cu(II);x=0,4,2and [M(Cefaz)y.Cl.H2O].xH2O where M = Fe(II), Co(II), Zn(II); y = 1; x=0,3,2 and M = Fe(III); y = 2; x = 3 .The complexes have been characterized on the basis of elemental analyses, IR, electronic and mass spectroscopy. The thermal behavior of the complexes was followed by thermo gravimetric analysis (TG) and differential thermogravimetry (DTG). The IR spectra showed that the ligand acts in a mononegative bidentate fashion. Preliminary pharmacological tests on cefazolin salt and its complexes exhibited some antimicrobial activity.
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