WAHDAN, K., Zarie, E., Elbialy, Z., Wahba, A., Heakal, B., Said, A. (2022). Antimicrobial and antioxidant evaluation of newly synthesized nanomaterials of potential anticorrosion properties based on Co (II), Ni (II), Cu (II) and Zn (II) nano complexes of N-(p-methyl phenyl)-N'-Benzoyl thiourea. test, 65(132), 1253-1268. doi: 10.21608/ejchem.2022.145699.6346
KHALID MARZOUK WAHDAN; Eman Said Zarie; Zaghloul Ibrahim Elbialy; Ali Mustafa Hassan Wahba; Bassem H. Heakal; Ahmed Osman Said. "Antimicrobial and antioxidant evaluation of newly synthesized nanomaterials of potential anticorrosion properties based on Co (II), Ni (II), Cu (II) and Zn (II) nano complexes of N-(p-methyl phenyl)-N'-Benzoyl thiourea". test, 65, 132, 2022, 1253-1268. doi: 10.21608/ejchem.2022.145699.6346
WAHDAN, K., Zarie, E., Elbialy, Z., Wahba, A., Heakal, B., Said, A. (2022). 'Antimicrobial and antioxidant evaluation of newly synthesized nanomaterials of potential anticorrosion properties based on Co (II), Ni (II), Cu (II) and Zn (II) nano complexes of N-(p-methyl phenyl)-N'-Benzoyl thiourea', test, 65(132), pp. 1253-1268. doi: 10.21608/ejchem.2022.145699.6346
WAHDAN, K., Zarie, E., Elbialy, Z., Wahba, A., Heakal, B., Said, A. Antimicrobial and antioxidant evaluation of newly synthesized nanomaterials of potential anticorrosion properties based on Co (II), Ni (II), Cu (II) and Zn (II) nano complexes of N-(p-methyl phenyl)-N'-Benzoyl thiourea. test, 2022; 65(132): 1253-1268. doi: 10.21608/ejchem.2022.145699.6346

Antimicrobial and antioxidant evaluation of newly synthesized nanomaterials of potential anticorrosion properties based on Co (II), Ni (II), Cu (II) and Zn (II) nano complexes of N-(p-methyl phenyl)-N'-Benzoyl thiourea

Egyptian Journal of Chemistry
Volume 65, Issue 132, December 2022, Pages 1253-1268    PDF (1.97 M)
Document Type: Original Article
DOI: 10.21608/ejchem.2022.145699.6346
Authors
KHALID MARZOUK WAHDAN1; Eman Said Zarie* 2; Zaghloul Ibrahim Elbialy3; Ali Mustafa Hassan Wahba4; Bassem H. Heakal3; Ahmed Osman Said5
1Chemistry department, faculty of Science, Al Azhar university , Cairo , Egypt
2Department of Therapeutic Chemistry, Institute of pharmaceutical Science and drug Industries Research , National Research Centre
3Egyptian Organization for Standardization and Quality
4Al Azhar University
5Senior researcher chemist, Greater Cairo Water Company, Cairo,
Abstract
Abstract

Microwave and traditional methods were used to synthesis a novel derivative of the thiourea ligand N-(p-methylphenyl)-N'-Benzoyl thiourea (MBT) and its transition metal complexes of Co (II), Ni (II), Cu (II), and Zn (II). Elemental analysis, FT-IR, mass spectroscopy, 1HNMR, 13CNMR, and UV-Visible were used to investigate the structure of MBT ligand and their complexes. Geometry of proposed chelate complexes was studied using electronic spectra, electron spin resonance (ESR), and magnetic susceptibility. Thermal gravimetric analysis (TGA) was used to study the solidity of complexes. X- ray diffraction XRD was used to investigate the surface morphologies of solid complexes. Antimicrobial activity of MBT ligand and their complexes was investigated. Also proposed chelate complexes were examined in vitro by radical scavenging activity (DPPH) to evaluate their antioxidant activity. The anticorrosion activity of the ligand was studied by weight loss method
Keywords
microwave-assisted synthesis; Thiourea derivative; antibacterial and antifungal activity; DPPH radical scavenging and anticorrosion activity
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