Synthesis and Antimicrobial Activity of Novel Bisbenzoxazine Monomer | ||
| Sohag Journal of Sciences | ||
| Volume 9, Issue 1, March 2024, Pages 1-6 PDF (559.07 K) | ||
| Document Type: Regular Articles | ||
| DOI: 10.21608/sjsci.2023.218511.1088 | ||
| Authors | ||
| Ahmed Soliman1; Kamal I Aly2; Amer A Amer1; Ahmed E Abdel-Aziz3; Mohamed Gamal Mohamed* 2, 4; Mostafa Rabie Belal* 1 | ||
| 1Department of Chemistry, Faculty of Science, Sohag University, Sohag 82524, Egypt. | ||
| 2Polymer Research Laboratory, Chemistry Department, Faculty of Science, Assiut University, Assiut 71516, Egypt. | ||
| 3Department of Botany and Microbiology, Faculty of Science, New Valley University, El-Kharga 72511, Egypt. | ||
| 4Department of Materials and Optoelectronic Science, College of Semiconductor and Advanced Technology Research, Center for Functional Polymers and Supramolecular Materials, National Sun Yat-Sen University, Kaohsiung, 804, Taiwan. | ||
| Abstract | ||
| In this research, a compound called 2,2'-((1E,1'E)-(hexane-1,6-diylbis(azanylylidene))bis(methanylylidene))diphenol (SA-HMDASF) was synthesized by combining salicylaldehyde and hexamethylene diamine. The resulting SA-HMDASF was then reduced using sodium borohydride, leading to the formation of 2,2'-((hexane-1,6-diylbis((SA-HMDA-NH) through a chemical reaction. Subsequently, SA-HMDA-NH was reacted with formaldehyde, resulting in the production of a benzoxazine monomer called SA-HMDA-BZ. To determine the chemical composition of SA-HMDA-BZ, different analytical methods such as FT-IR, 1H, and 13C NMR spectroscopy were employed. These methods were crucial in identifying and confirming the molecular composition and arrangement of the compound. Furthermore, Scanning Electron Microscopy (SEM) was used to analyze the surface morphology of SA-HMDA-BZ while its crystalline properties were assessed through X-ray Diffraction (XRD) analysis. These characterization techniques provided valuable insights into the physical attributes and structural properties of SA-HMDA-BZ. Additionally, the antimicrobial activity of SA-HMDA-BZ was investigated, and the results displayed promising outcomes. The compound exhibited notable antimicrobial properties, suggesting its potential as an effective agent against various microorganisms. | ||
| Keywords | ||
| Benzoxazine; Crystallinity; Thermal stability and Antimicrobial activity | ||
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