Synthesis and Characterization of Linear Thermally Stable polyester contain Schiff Bases | ||
| Egyptian Journal of Chemistry | ||
| Article 18, Volume 63, Issue 8, August 2020, Pages 2999-3013 PDF (1.26 M) | ||
| Document Type: Original Article | ||
| DOI: 10.21608/ejchem.2020.25217.2526 | ||
| Authors | ||
| Ahmed M Abbas* 1; Ayman Saeed Mohammed Taib2; Noor H.M. Saeed3 | ||
| 1Department of Chemistry, College of Science, University of Misan, Maysan, Iraq | ||
| 2Department of Chemistry, College of Education For Pure Sciences, University of Mosul, Mosul, Iraq | ||
| 3Department of Chemistry, College of Education for pure science, University of Mosul,Mosul, Iraq | ||
| Abstract | ||
| A copolymers are important compounds today because of their wide applications in various industrial and medical fields and in other fields. Therefore, the study of preparing many of these polymers has been studied. This research involved preparing linear polyester contain Schiff-base unit by interfacial polycondensation three type diacid chloride (Succinoyl Chloride, Adipoyl Chloride and sebacoyl Chloride) in a chloroform /water system employing phase transfer catalyst with monomer containing two hydroxyl which is derived from a 4-hydroxy aniline reacted with a 4-hydroxy benzaldehyde monomer. The monomer (EM1) and polyester (EM2, EM3, and EM4) were characterized by FTIR, 1H NMR, 13C NMR and TGA analysis. The polyester–Schiff base so obtained show good thermal stability. | ||
| Keywords | ||
| polyester; Schiff baes; interfacial polycondensation; phase transfer catalyst; FTIR; 1H NMR; 13C NMR and TGA analysis | ||
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