New biopolymer nanocomposites-based Polycaprolactone /polybutylene succinate modified clay: preparation and characterization | ||
| Egyptian Journal of Chemistry | ||
| Article 17, Volume 64, Issue 8, August 2021, Pages 4137-4142 PDF (432.44 K) | ||
| Document Type: Original Article | ||
| DOI: 10.21608/ejchem.2021.70258.3548 | ||
| Authors | ||
| Manar Ghyath Abd-Almutalib Al-Mosawy* ; Ammar kareem madlol; Kawther Mejbel Hussein | ||
| Medical Laboratory Techniques Department, Imam Ja'afar Al-Sadiq University, Al-Najaf, Iraq. | ||
| Abstract | ||
| (Polybutylin succinate)PBS / (Polycaprolactone)PCL and AZO from organic clays incorporating2-(diethylamino)ethyl 3-((4-acetylphenyl)diazenyl)-4-aminobenzoate montmorillonite (AZO-MMT) were used to produce polymer compounds by mixing the solution. These materials have been characterized using X-ray diffraction, infrared spectroscopy (FTIR), thermogravimetric analysis (TGA) and transmission electron microscopy (TEM). The nanocomposites have shown increased thermal stability. Where the results obtained from the XRD indicate that the materials prepared in this research are nanocomposites. The results of TEM were confirmed by the insertion of the nanocomposite. In addition, the solution molding process was used to prepare these nanocomposites, and these results were distinguished for comparison with the above-mentioned process. | ||
| Keywords | ||
| Na- montmorillonite; Polycaprolactone; Polybutylene succinate; nanocomposite; procaine; 4-aminoacetophenone | ||
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